System: Ethanol - Water
Description of the exercise:
Question 1: Do a distillation with total reflux and estimate average plate efficiency as a function of vapor speed.
Question 2: Measure the pressure drop over the column for different vapor speeds and find capacity borders (lower and higher).
Question 3: Do a ‘binary-batch’ distillation with given reflux and reboiler duty. Decide distillate composition as a function of n/n0.
n = total number of moles back in reboiler + column.
n0 = total number of moles at the beginning of the experiment.
Compare experimental results with calculations
Version 1: Questions 1, 2
Short report (2-3 pages)
1 day for experiments
Version 2: Whole exercise (Questions 1, 2, 3).
Short report (3-5 pages)
2 days for experiments
Version 3: Whole exercise (Questions 1, 2, 3).
Long report (~ 20pages)
2 days for experiments